2,4-二叔丁氧基嘧啶-5-硼酸合成路线 (共 3 条)
反应条件
n-butyllithium; boron triethoxide in tetrahydrofuran T=-100°C;
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 225 - 230
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate
1.) DME, 10 min, 2.) DME, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wellmar, Ulf; Hoernfeldt, Anna-Britta; Gronowitz, Salo
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 2 p. 409 - 414
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate
1.) DME, 10 min, 2.) DME, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wellmar, Ulf; Hoernfeldt, Anna-Britta; Gronowitz, Salo
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 2 p. 409 - 414