4-(4-溴-苯基)-硫代吗啉 1,1-二氧化物合成路线 （共 4 条）
反应条件
sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in toluene T=80°C;
参考文献
IRM LLC; CHE, Jianwei; DING, Qiang; HE, Xiaohui; LIU, Hong; LIU, Yahua; MICHELLYS, Pierre-Yves; OKRAM, Barun; WU, Xu; YANG, Kunyong; ZHU, Xuefeng
Patent: WO2011/14795 A2, 2011 ;
Location in patent: Page/Page column 91 ;
WO 2011/014795 A2
反应条件
boric acid; glycerol in water T=100°C; Michael Addition; 18 h; Green chemistry;
参考文献
Halimehjnai, Azim Ziyaei; Hosseyni, Seyedmorteza; Gholami, Hadi; Hashemi, Mohammed M.
Synthetic Communications, 2013 , vol. 43, # 2 p. 191 - 197,7
反应条件
indium; ammonium chloride; acetic acid in methanol; water aza-Michael type 1,4-addition reaction; 24 h; Inert atmosphereReflux;
参考文献
Han, Joon Hee; Choi, Jaehwan; Jun, Young Moo; Lee, Byung Min; Kim, Byeong Hyo
Heterocycles, 2010 , vol. 81, # 2 p. 317 - 327
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide T=90°C;
参考文献
WO2011/14795 A2, ;
Page/Page column 91-92 ;
WO 2011/014795 A2
