6-氯-2-(氯甲基)烟酸甲酯合成路线 （共 3 条）
反应条件
trichlorophosphate 3 h; Reflux;
参考文献
WO2010/11375 A2, ;
Page/Page column 51-52 ;
WO 2010/011375 A2
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: trichlorophosphate / 3 h / 20 °C / |Inert atmosphere; |Reflux 3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 0 - 20 °C / |Inert atmosphere 4: trichlorophosphate / 3 h / 20 °C / |Inert atmosphere; |Reflux View Scheme
反应条件
1: trichlorophosphate / 3 h / 20 °C / |Inert atmosphere; |Reflux 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 0 - 20 °C / |Inert atmosphere 3: trichlorophosphate / 3 h / 20 °C / |Inert atmosphere; |Reflux View Scheme
