反应条件
1: 6-fluoro-3-{4-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1H-1,2,3-triazol-1-yl}-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one With sodium hydride in N,N-dimethyl-formamide; mineral oil T=0°C; 0.5 h; 2: trifluoromethylsulfonyloxy-2,2,2-trifluoroethane in N,N-dimethyl-formamide; mineral oil T=20°C;
参考文献
MERCK and CO., INC.
Patent: WO2008/156580 A1, 2008 ;
Location in patent: Page/Page column 43-44 ;
WO 2008/156580 A1