(r)-2-甲苯磺酰氧基丙酸甲酯合成路线 (共 3 条)
反应条件
pyridine in dichloromethane T=20°C; 6 h;
参考文献
Perrone, Maria Grazia; Santandrea, Ernesto; Bleve, Laura; Vitale, Paola; Colabufo, Nicola Antonio; Jockers, Ralf; Milazzo, Ferdinando Maria; Sciarroni, Anna Floriana; Scilimati, Antonio
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 5 p. 2473 - 2488
反应条件
N-Trimethylamine hydrochloride; triethylamine in acetonitrile T=5°C; 0.333333 h;
参考文献
Bonnert, Roger Victor; Luker, Timothy Jon; Patel, Anil; Rigby, Aaron
Patent: US2009/12151 A1, 2009 ;
Location in patent: Page/Page column 8 ;
反应条件
chiral stationary phase derived from aminated silica gel, L-2-(p-toluenesulfonamido)-3-phenylpropionyl chloride and dendrimer in methanol; water T=25°C; Resolution of racemate;
参考文献
He, Bao-Jiang; Yin, Chuan-Qi; Li, Shi-Rong; Bai, Zheng-Wu
Chirality, 2010 , vol. 22, # 1 p. 69 - 76