1,1-亚甲基-2-萘酚合成路线 (共 81 条)
反应条件
1: With 2-amino-2-methyl-propan-1-ol in methanol Condensation; 3 h; Heating; 2: With sodium tetrahydroborate in methanol T=0 - 20°C; Dimerization; reduction; 3.5 h;
参考文献
Rao, P. Venkateshwara; Rao, Chebrolu Pulla; Wegelius, Elina K.; Kolehmainen, Erkki; Rissanen, Kari
Journal of the Chemical Society - Dalton Transactions, 1999 , # 24 p. 4469 - 4474
反应条件
hydrogen bromide in water; acetonitrile T=20°C; Friedel-Crafts Alkylation; 5 h;
参考文献
Xu, Cong; Yuan, Hongjuan; Liu, Yingjie; Wang, Mang; Liu, Qun
RSC Advances, 2014 , vol. 4, # 4 p. 1559 - 1562
反应条件
sulfuric acid in tetrahydrofuran T=40°C; 1.16667 h;
参考文献
Kito, Taketoshi; Yoshinaga, Kohji; Yamaya, Makoto; Mizobe, Hoyou
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3336 - 3339
反应条件
1: 1,1-dibromomethane With diethylamine T=55°C; 1.5 h; 2: β-naphthol in dichloromethane T=100°C; 27 h;
参考文献
Hon, Yung-Son; Chou, Yu-Yu; Wu, I-Che
Synthetic Communications, 2004 , vol. 34, # 12 p. 2253 - 2267
反应条件
in acetic acid T=90°C; 2 h;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 47, # 9 p. 543 - 556
反应条件
1: 46 percent 2: 38 percent / toluene / 2 h / Heating View Scheme
参考文献
Archiv der Pharmazie, , vol. 325, # 11 p. 695 - 700
反应条件
in toluene 2 h; Heating;
参考文献
Archiv der Pharmazie, , vol. 325, # 11 p. 695 - 700
反应条件
1: 67 percent / methanol / 20 °C 2: boric oxide / methanol View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 592, # 2 p. 180 - 193
反应条件
potassium hydroxide T=220 - 240°C;
参考文献
Monatshefte fuer Chemie, , vol. 73, p. 45,48
反应条件
in toluene 2 h; Heating;
参考文献
Archiv der Pharmazie, , vol. 325, # 11 p. 695 - 700