4-乙酰苯基三氟甲烷磺酸酯合成路线 (共 140 条)
反应条件
triethylamine T=-40°C; 0.25 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 8 p. 2076 - 2080
反应条件
potassium carbonate in tetrahydrofuran T=120°C; 0.1 h; Microwave irradiation;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 1 p. 137 - 140
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Tetrahedron, , vol. 61, # 3 p. 709 - 715
反应条件
pyridine in dichloromethane T=20°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 36 p. 8864 - 8865
反应条件
1: in tetrachloromethane T=-10°C; 0.0833333 h; 2: With cesium fluoride in tetrachloromethane T=-10°C; 0.0833333 h; 3: in tetrachloromethane T=90°C; 0.0166667 h;
参考文献
Journal of Fluorine Chemistry, , vol. 107, # 2 p. 321 - 327
反应条件
1: 13 percent Chromat. / Zn; allyl chloride; TFA / CoBr2(2,2'-bipyridine) / acetonitrile; pyridine; dodecane / 8 h / 50 °C 2: pyridine / 0 - 20 °C View Scheme
参考文献
Synlett, , # 6 p. 881 - 884
反应条件
1: With cesium fluoride in tetrachloromethane T=-10°C; 0.166667 h; 2: in tetrachloromethane T=90°C; 1 h;
参考文献
Journal of Fluorine Chemistry, , vol. 107, # 2 p. 321 - 327
反应条件
cesium fluoride in various solvent(s) T=45°C; 1 h; Product distribution; Further Variations:Temperatures;
参考文献
Journal of Fluorine Chemistry, , vol. 107, # 2 p. 321 - 327
反应条件
palladium diacetate; 1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine 1.) DMF, 80 deg C, 24 h, 2.) DMF, 80 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7858 - 7862
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772