4-乙酰苯基三氟甲烷磺酸酯合成路线 （共 140 条）
反应条件
triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in propan-1-ol
Suzuki cross-coupling reaction; 3 h; Heating;
参考文献
Molander, Gary A.; Rivero, Marta Rodriguez
Organic Letters, 2002 , vol. 4, # 1 p. 107 - 109
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran
3 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
反应条件
lithium chloride; tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane in various solvent(s)
2 h; Ambient temperature;
参考文献
Farina, Vittorio; Krishnan, Bala
Journal of the American Chemical Society, 1991 , vol. 113, # 25 p. 9585 - 9595
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl acetamide
T=60°C; P=775.743 Torr; 12 h;
参考文献
Saini, Vaneet; Liao, Longyan; Wang, Qiaofeng; Jana, Ranjan; Sigman, Matthew S.
Organic Letters, 2013 , vol. 15, # 19 p. 5008 - 5011
反应条件
3,4-dihydroxy-1-tert-butylbenzene; palladium in 1,4-dioxane
T=23°C; 24 h; variation of reaction conditions; Product distribution;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5478
反应条件
1: trimethylsilylacetylene With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C;
2: With indium(III) chloride in tetrahydrofuran; hexane
T=-78 - 20°C;
3: 4-acetylphenyl triflate With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane
1 h; Heating; Further stages.;
参考文献
Perez, Ignacio; Sestelo, Jose Perez; Sarandeses, Luis A.
Organic Letters, 1999 , vol. 1, # 8 p. 1267 - 1269
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran
1 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
反应条件
N-ethyl-N,N-diisopropylamine; 1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane
T=85°C; Heck coupling; 1.75 h;
参考文献
Hansen, Anders Lindhardt; Skrydstrup, Troels
Journal of Organic Chemistry, 2005 , vol. 70, # 15 p. 5997 - 6003
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; caesium carbonate in tetrahydrofuran
Suzuki-Miyaura reaction; 72 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo; Ribagorda, Maria; Biolatto, Betina
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5534 - 5539
反应条件
polymethylhydrosiloxane; cesium fluoride; copper(l) chloride; bis-triphenylphosphine-palladium(II) chloride in 1-methyl-pyrrolidin-2-one
T=20°C; Sonogashira reaction; 5 h;
参考文献
Gallagher, William P.; Maleczka Jr., Robert E.
Synlett, 2003 , # 4 p. 537 - 541
