4-乙酰苯基三氟甲烷磺酸酯合成路线 (共 140 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Pena-Lopez, Miguel; Ayan-Varela, Miguel; Sarandeses, Luis A.; Perez Sestelo, Jose
Chemistry - A European Journal, 2010 , vol. 16, # 32 p. 9905 - 9909
反应条件
pyridine; 2,6-di-tert-butyl-4-methyl-phenol; pyridine hydrogenfluoride; lithium chloride; tetrakis(triphenylphosphine) palladium(0) 1.) 1,4,-dioxane, reflux, 31 h, 2.) THF, 23 deg C, 16 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5478
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
trifuran-2-yl-phosphane; bis(benzonitrile)palladium(II) dichloride in various solvent(s) T=100°C; 5 h;
参考文献
Farina, Vittorio; Kapadia, Suresh; Krishnan, Bala; Wang, Chenjie; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 5905 - 5911
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane T=65°C; 40 h; also with other reagents; Rate constantProduct distribution;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate in N,N-dimethyl-formamide T=70°C; 3.5 h;
参考文献
Gerlach, Uwe; Wollmann, Theo
Tetrahedron Letters, 1992 , vol. 33, # 38 p. 5499 - 5502
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 20 p. 5434 - 5444
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 6 h;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450