4-乙酰苯基三氟甲烷磺酸酯合成路线 （共 140 条）
反应条件
1: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 2: 67 percent / dimethylformamide / Ambient temperature; electrolysis 3: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
1: 84 percent / polymethylhydrosiloxane; CsF; CuCl / PdCl2(PPh3)2 / 1-methyl-pyrrolidin-2-one / 5 h / 25 °C 2: 78 percent / potassium carbonate; 18-crown-6 / toluene / 8 h / 120 °C View Scheme
参考文献
Gallagher, William P.; Maleczka Jr., Robert E.
Synlett, 2003 , # 4 p. 537 - 541
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium acetate in tetrahydrofuran Suzuki-Miyaura cross-coupling; RefluxInert atmosphere;
参考文献
Wang, Bing; Sun, Hui-Xia; Sun, Zhi-Hua
European Journal of Organic Chemistry, 2009 , # 22 p. 3688 - 3692
反应条件
tetrabutylammomium bromide; potassium carbonate; quasi polymeric 4-pyridine-aldoxime Pd(II)-catalyst T=120°C; Suzuki-Miyaura reaction; 0.333333 h; microwave irradiation;
参考文献
Solodenko, Wladimir; Schoen, Uwe; Messinger, Josef; Glinschert, Anja; Kirschning, Andreas
Synlett, 2004 , # 10 p. 1699 - 1702
反应条件
1: methyllithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 4-acetylphenyl triflate With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 4.5 h; Heating; Further stages.;
参考文献
Organic Letters, , vol. 1, # 8 p. 1267 - 1269
反应条件
tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane; lithium chloride in various solvent(s) T=60°C;
参考文献
Journal of the American Chemical Society, , vol. 113, # 25 p. 9585 - 9595
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 4.5 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 123, # 18 p. 4155 - 4160
反应条件
potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water Suzuki coupling reaction; 18 h; Heating;
参考文献
Tetrahedron, , vol. 58, # 8 p. 1465 - 1470
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C;
参考文献
Journal of Organic Chemistry, , vol. 58, # 20 p. 5434 - 5444
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; water; caesium carbonate in tetrahydrofuran Suzuki coupling reaction; 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 14 p. 5534 - 5539
