4-乙酰苯基三氟甲烷磺酸酯合成路线 （共 140 条）
反应条件
3,4-dihydroxy-1-tert-butylbenzene; palladium in 1,4-dioxane T=23°C; 24 h; variation of reaction conditions; Product distribution;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5478
反应条件
tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; lithium chloride in various solvent(s) T=60°C; 48 h; other alkyltin compounds; var. phosphines and arsines; Rate constantProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 113, # 25 p. 9585 - 9595
反应条件
ammonium hydroxide; 2,6-di-tert-butyl-4-methyl-phenol; lithium chloride; tetrakis(triphenylphosphine) palladium(0) 1.) 1,4-dioxane, reflux, 16 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 5478
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane; [Fe(II)(C5H5)(C5H4PPh2)] in 1,4-dioxane T=80°C; 14 h;
参考文献
Nising, Carl F.; Schmid, Ulrike K.; Nieger, Martin; Braese, Stefan
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6830 - 6833
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; caesium carbonate in tetrahydrofuran Suzuki-Miyaura reaction; 72 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo; Ribagorda, Maria; Biolatto, Betina
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5534 - 5539
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; caesium carbonate in tetrahydrofuran Suzuki-Miyaura reaction; 72 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo; Ribagorda, Maria; Biolatto, Betina
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5534 - 5539
反应条件
pyridine; 2,6-di-tert-butyl-4-methyl-phenol; hexamethyl-distannane; pyridine hydrogenfluoride; lithium chloride; tetrakis(triphenylphosphine) palladium(0) 1.) 1,4-dioxane, reflux, 24 h, 2.) THF, 23 deg C, 16 h; Yield given. Multistep reaction;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5478
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; zinc; Co(2,2'-bipyridine)Br2 in pyridine; N-dodecane; acetonitrile T=50°C; 1 h; Title compound not separated from byproducts;
参考文献
Synlett, , # 6 p. 881 - 884
反应条件
1: Pd2(dba)3, BINAP, Cs2CO3 / tetrahydrofuran / 4 h / 65 °C 2: 2.0M HCl / tetrahydrofuran View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 36 p. 6367 - 6370
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; cross-coupling;
参考文献
Nishihara, Yasushi; Ikegashira, Kazutaka; Hirabayashi, Kazunori; Ando, Jun-Ichi; Mori, Atsunori; Hiyama, Tamejiro
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1780 - 1787
