4-乙酰苯基三氟甲烷磺酸酯合成路线 （共 140 条）
反应条件
NiII chloride hexahydrate; potassium bromide T=185 - 190°C; Arbuzov reaction; 20 h; Inert atmosphere;
参考文献
Yang, Guoqiang; Shen, Chaoren; Zhang, Liang; Zhang, Wanbin
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5032 - 5035
反应条件
palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in tetrahydrofuran T=65°C; 4 h;
参考文献
Ahman, Jens; Buchwald, Stephen L.
Tetrahedron Letters, 1997 , vol. 38, # 36 p. 6363 - 6366
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water 18 h; Heating;
参考文献
Molander; Ito
Organic letters, 2001 , vol. 3, # 3 p. 393 - 396
反应条件
tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; 2.5 h;
参考文献
Hatanaka, Yasuo; Hiyama, Tamejiro
Tetrahedron Letters, 1990 , vol. 31, # 19 p. 2719 - 2722
反应条件
potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water Suzuki coupling reaction; 18 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo
Tetrahedron, 2002 , vol. 58, # 8 p. 1465 - 1470
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water 18 h; Heating;
参考文献
Molander; Ito
Organic letters, 2001 , vol. 3, # 3 p. 393 - 396
反应条件
potassium carbonate in ethanol T=20 - 60°C; Suzuki-Miyaura reaction; 6 h; in air;
参考文献
Hagiwara, Hisahiro; Sasaki, Hirokazu; Tsubokawa, Norio; Hoshi, Takashi; Suzuki, Toshio; Tsuda, Tetsuya; Kuwabata, Susumu
Synlett, 2010 , # 13 p. 1990 - 1996
反应条件
1: phenyllithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 4-acetylphenyl triflate With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 6 h; Heating; Further stages.;
参考文献
Perez, Ignacio; Sestelo, Jose Perez; Sarandeses, Luis A.
Organic Letters, 1999 , vol. 1, # 8 p. 1267 - 1269
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
palladium diacetate in ethanol T=95°C; 0.25 h; microwave irradiation;
参考文献
Kabalka, George W.; Zhou, Li-Li; Naravane, Abhijit
Tetrahedron Letters, 2006 , vol. 47, # 38 p. 6887 - 6889
