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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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9-蒽丙酸乙酯
合成路线
（共 10 条）
3054-95-3
丙烯醛缩二乙醇
+
1564-64-3
9-溴蒽
→
反应条件
38982-12-6
9-蒽丙烯醛
+
109690-74-6
9-蒽丙酸乙酯
反应条件
sodium acetate; Pd(NH3)4/NaY zeolite in 1-methyl-pyrrolidin-2-one T=140°C; Heck reaction; 6 h;
参考文献
Noel, Sebastien; Luo, Ciahong; Pinel, Catherine; Djakovitch, Laurent
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1128 - 1140
3054-95-3
丙烯醛缩二乙醇
+
1564-64-3
9-溴蒽
→
反应条件
109690-74-6
9-蒽丙酸乙酯
反应条件
1: With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); sodium acetate in 1-methyl-pyrrolidin-2-one T=140°C; 6 h; 2: With hydrogenchloride; water in 1-methyl-pyrrolidin-2-one
参考文献
Noel, Sebastien; Djakovitch, Laurent; Pinel, Catherine
Tetrahedron Letters, 2006 , vol. 47, # 23 p. 3839 - 3842
61161-88-4
→
反应条件
109690-74-6
9-蒽丙酸乙酯
反应条件
water; sodium chloride in dimethyl sulfoxide T=130°C; 72 h;
参考文献
Bach, Anders; Eildal, Jonas N. N.; Stuhr-Hansen, Nicolai; Deeskamp, Rasmus; Gottschalk, Marie; Pedersen, Soren W.; Kristensen, Anders S.; Stromgaard, Kristian
Journal of Medicinal Chemistry, 2011 , vol. 54, # 5 p. 1333 - 1346
3984-22-3
2-乙烯基-1,3-二氧戊环
+
1564-64-3
9-溴蒽
→
反应条件
38982-12-6
9-蒽丙烯醛
+
109690-74-6
9-蒽丙酸乙酯
反应条件
tetra-n-butylammonium acetate; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=110°C; Heck arylation; 3 h;
参考文献
Pan, Ke; Noel, Sebastien; Pinel, Catherine; Djakovitch, Laurent
Journal of Organometallic Chemistry, 2008 , vol. 693, # 17 p. 2863 - 2868
3054-95-3
丙烯醛缩二乙醇
+
1564-64-3
9-溴蒽
→
反应条件
120-12-7
蒽
+
38982-12-6
9-蒽丙烯醛
+
109690-74-6
9-蒽丙酸乙酯
反应条件
tetra-n-butylammonium acetate; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=110°C; Heck arylation; 5 h;
参考文献
Pan, Ke; Noel, Sebastien; Pinel, Catherine; Djakovitch, Laurent
Journal of Organometallic Chemistry, 2008 , vol. 693, # 17 p. 2863 - 2868
64-17-5
乙醇
+
41034-83-7
3-(9-蒽基)丙酸
→
反应条件
109690-74-6
9-蒽丙酸乙酯
反应条件
sulfuric acid 5 h; Heating;
参考文献
Pietro, Cinzia Di; Campagna, Sebastiano; Ricevuto, Vittorio; Giannetto, Michele; Manfredi, Amedea; Pozzi, Gianluca; Quici, Silvio
European Journal of Organic Chemistry, 2001 , # 3 p. 587 - 594
24463-19-2
9-氯甲基蒽
→
反应条件
109690-74-6
9-蒽丙酸乙酯
反应条件
1: 72 percent / NaH / tetrahydrofuran / 15 h / 20 °C 2: 90 percent / NaOH / aq. ethanol / 0.5 h / 20 °C 3: 89 percent / 0.33 h / 220 °C 4: 94 percent / H2SO4 / 5 h / Heating View Scheme
参考文献
Pietro, Cinzia Di; Campagna, Sebastiano; Ricevuto, Vittorio; Giannetto, Michele; Manfredi, Amedea; Pozzi, Gianluca; Quici, Silvio
European Journal of Organic Chemistry, 2001 , # 3 p. 587 - 594
58353-42-7
→
反应条件
109690-74-6
9-蒽丙酸乙酯
反应条件
1: 89 percent / 0.33 h / 220 °C 2: 94 percent / H2SO4 / 5 h / Heating View Scheme
参考文献
Pietro, Cinzia Di; Campagna, Sebastiano; Ricevuto, Vittorio; Giannetto, Michele; Manfredi, Amedea; Pozzi, Gianluca; Quici, Silvio
European Journal of Organic Chemistry, 2001 , # 3 p. 587 - 594
75-03-6
碘乙烷
→
反应条件
109690-74-6
9-蒽丙酸乙酯
反应条件
暂无反应条件数据
参考文献
Stewart,F.H.C.
Australian Journal of Chemistry, 1960 , vol. 13, p. 478 - 487
109690-74-6
9-蒽丙酸乙酯
→
反应条件
22689-05-0
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Heating;
参考文献
Pietro, Cinzia Di; Campagna, Sebastiano; Ricevuto, Vittorio; Giannetto, Michele; Manfredi, Amedea; Pozzi, Gianluca; Quici, Silvio
European Journal of Organic Chemistry, 2001 , # 3 p. 587 - 594
