乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
T=100°C; Wittig olefination; 0.166667 h; Title compound not separated from byproducts.;
参考文献
Thiemann, Thies; Watanabe, Masataka; Tanaka, Yasuko; Mataka, Shuntaro
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 578 - 584
反应条件
hollandite in toluene T=110°C; Wittig Olefination; 4 h; Catalytic behavior; diastereoselective reaction;
参考文献
Kona, Jagadeswara R.; King'Ondu, Cecil K.; Howell, Amy R.; Suib, Steven L.
ChemCatChem, 2014 , vol. 6, # 3 p. 749 - 752
反应条件
Wittig olefination; Title compound not separated from byproducts.;
参考文献
Craig, Donald; Slavov, Nikolay K.
Chemical Communications, 2008 , # 45 p. 6054 - 6056
参考文献
Rokade, Balaji V.; Malekar, Sanjeev K.; Prabhu, Kandikere Ramaiah
Chemical Communications, 2012 , vol. 48, # 44 p. 5506 - 5508
反应条件
1: 4-chloro-benzylamine With palladium on activated charcoal T=170°C; 3 h; Irradiationmicrowave; 2: ethyl (triphenylphosphoranylidene)acetate in water T=20°C; Wittig reaction; 12 h; 3: With hydrogen in water T=20°C; 8 h;
参考文献
Chandrasekhar; Pavan Kumar Reddy; Nagesh; Raji Reddy
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1269 - 1271
反应条件
1: benzyl-methyl-amine With palladium on activated charcoal T=170°C; 3 h; Irradiationmicrowave; 2: ethyl (triphenylphosphoranylidene)acetate in water T=20°C; Wittig reaction; 12 h; 3: With hydrogen in water T=20°C; 8 h;
参考文献
Chandrasekhar; Pavan Kumar Reddy; Nagesh; Raji Reddy
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1269 - 1271
反应条件
1: benzylamine With palladium on activated charcoal T=170°C; 3 h; Irradiationmicrowave; 2: ethyl (triphenylphosphoranylidene)acetate in water T=20°C; Wittig reaction; 12 h; 3: With hydrogen in water T=20°C; 8 h;
参考文献
Chandrasekhar; Pavan Kumar Reddy; Nagesh; Raji Reddy
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1269 - 1271
反应条件
1: N-Benzylbenzylamine With palladium on activated charcoal T=170°C; 3 h; Irradiationmicrowave; 2: ethyl (triphenylphosphoranylidene)acetate in water T=20°C; Wittig reaction; 12 h; 3: With hydrogen in water T=20°C; 8 h;
参考文献
Chandrasekhar; Pavan Kumar Reddy; Nagesh; Raji Reddy
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1269 - 1271
反应条件
hydrogen; sodium acetate; pyridinium chlorochromate; nickel Yield given. Multistep reaction;
参考文献
Anderson, Robert C.; Fraser-Reid, B.
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4786 - 4790
反应条件
triphenylphosphine in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 2 p. 283 - 290
