乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
反应条件
aluminum oxide T=25°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dhavale, Dilip D.; Sindkhedkar, Milind D.; Mali, Raghao S.
Journal of Chemical Research, Synopses, 1995 , # 10 p. 414 - 415
反应条件
in benzene Wittig reaction; Reflux;
参考文献
Jin, Yun-Zhou; Fu, Da-Xu; Ma, Nan; Li, Zhan-Cheng; Liu, Quan-Hai; Xiao, Lin; Zhang, Rong-Hua
Molecules, 2011 , vol. 16, # 11 p. 9368 - 9385
反应条件
in dichloromethane T=23°C; 2 h; Inert atmosphere;
参考文献
Sanchez-Larios, Eduardo; Holmes, Janice M.; Daschner, Crystal L.; Gravel, Michel
Synthesis, 2011 , # 12 art. no. C29911SS, p. 1896 - 1904
反应条件
1: in toluene T=20°C; Wittig reaction; 2: With triphenylphosphine; [MoO2Cl2(dmf)2] in toluene 24 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 4-5 p. 713 - 718
反应条件
in benzene 54 h; Heating;
参考文献
Brubaker; DeRuiter; Whitmer
Journal of Medicinal Chemistry, 1986 , vol. 29, # 6 p. 1094 - 1099
反应条件
manganese(IV) oxide in toluene Oxidation; Wittig reaction; 24 h; Heating;
参考文献
Blackburn, Leonie; Wei, Xudong; Taylor, Richard J. K.
Chemical Communications, 1999 , # 14 p. 1337 - 1338
反应条件
in benzene T=20°C; Wittig reaction;
参考文献
Srinivas; Sai Pavan Kumar; China Raju; Jayathirtha Rao; Naidu; Ramakrishna; Diwan, Prakash V.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 20 p. 5915 - 5918
反应条件
T=100°C; Wittig olefination; 0.166667 h; Title compound not separated from byproducts.;
参考文献
Thiemann, Thies; Watanabe, Masataka; Tanaka, Yasuko; Mataka, Shuntaro
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 578 - 584
反应条件
in dichloromethane 2 h; Ambient temperature;
参考文献
Morisaki; Funabashi; Furukawa; Shimazawa; Kanematsu; Ando; Okuda; Iwasaki
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 11 p. 2945 - 2953
反应条件
sodium acetate; pyridinium chlorochromate in dichloromethane oxidation-Wittig reaction; 3.5 h;
参考文献
Shet, Jyoti; Desai, Vidya; Tilve, Santosh
Synthesis, 2004 , # 11 p. 1859 - 1863