乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
1: 2-(aminomethyl)naphthalene With palladium on activated charcoal T=170°C; 3 h; Irradiationmicrowave; 2: ethyl (triphenylphosphoranylidene)acetate in water T=20°C; Wittig reaction; 12 h; 3: With hydrogen in water T=20°C; 8 h;
参考文献
Chandrasekhar; Pavan Kumar Reddy; Nagesh; Raji Reddy
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1269 - 1271
反应条件
in ethanol; palladium; acetonitrile
参考文献
Sankyo Company, Limited
Patent: US5556864 A1, 1996 ;
US 5556864 A
反应条件
in xylene 12 h; Heating;
参考文献
Deshmukh, R. S. Konde; Paradkar, M. V.
Synthetic Communications, 1988 , vol. 18, # 6 p. 589 - 596
反应条件
in tetrahydrofuran; ethyl acetate; toluene
参考文献
Merck Frosst Canada, Inc.
Patent: US5334597 A1, 1994 ;
US 5334597 A
反应条件
in acetonitrile T=190°C; 0.333333 h; microwave heating;
参考文献
Wu, Jinlong; Wu, Huafeng; Wei, Shaoyong; Dai, Wei-Min
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4401 - 4404
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide T=230°C; 0.333333 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Wu, Jinlong; Wu, Huafeng; Wei, Shaoyong; Dai, Wei-Min
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4401 - 4404
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Castellano, Sabrina; Fiji, Hannah D. G.; Kinderman, Sape S.; Watanabe, Masaru; De Leon, Pablo; Tamanoi, Fuyuhiko; Kwon, Ohyun
Journal of the American Chemical Society, 2007 , vol. 129, # 18 p. 5843 - 5845
参考文献
FMC Corporation
Patent: US4883789 A1, 1989 ;
反应条件
manganese(IV) oxide in dichloromethane T=20°C; 0.0833333 h; Product distribution; Further Variations:Temperaturestime;
参考文献
Runcie, Karen A.; Taylor, Richard J. K.
Chemical Communications, 2002 , # 9 p. 974 - 975
反应条件
in toluene T=90°C; optical yield given as percent de;
参考文献
Zhou, Feng; Yang, Miao; Lu, Xiyan
Organic Letters, 2009 , vol. 11, # 6 p. 1405 - 1408
