乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
反应条件
water; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate in tetrahydrofuran -30 deg C, 30 min; -30 deg C to RT;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 1994 , vol. 35, # 48 p. 8951 - 8954
反应条件
N,N-dimethyl-formamide 15 h; Reflux;
参考文献
Boulos, Leila S.; Abdel-Malek, Hoda A.; El-Sayed, Naglaa F.; Moharam, Maysa E.
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 2 p. 225 - 237
反应条件
1: 60 percent / benzene / Heating 2: 230 °C / 5 Torr View Scheme
参考文献
Abdou, Wafaa M.; Ganoub, Neven A. F.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 60, # 1.2 p. 49 - 55
反应条件
in toluene 10 h; Reflux;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 66, # 10 p. 1056 - 1068
反应条件
in toluene Reflux; Mechanism;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 66, # 10 p. 1056 - 1068
反应条件
in dichloromethane
T=20°C; Wittig condensation; 24 h; stereoselective reaction;
参考文献
Viton, Florian; Landreau, Cyrille; Rustidge, David; Little, Gill; Robert, Fabien; Williamson, Gary; Barron, Denis
Journal of Labelled Compounds and Radiopharmaceuticals, 2010 , vol. 53, # 5-6 p. 371 - 374
反应条件
N,N-diethylaniline
Wittig reaction; 4 h; Reflux;
参考文献
Khoobi, Mehdi; Alipour, Masoumeh; Zarei, Samaneh; Jafarpour, Farnaz; Shafiee, Abbas
Chemical Communications, 2012 , vol. 48, # 24 p. 2985 - 2987
反应条件
in diphenylether
Wittig reaction; 0.333333 h; Reflux;
参考文献
Patre, Rupesh E.; Shet, Jyoti B.; Parameswaran, Perunninakulath S.; Tilve, Santosh G.
Tetrahedron Letters, 2009 , vol. 50, # 47 p. 6488 - 6490
反应条件
in dichloromethane; N,N-dimethyl-formamide
T=20°C; 20 h;
参考文献
Cho, Joong-Heui; Jung, Kwan-Young; Jung, Younghwan; Kim, Min Hye; Ko, Hyojin; Park, Chul-Seung; Kim, Yong-Chul
European Journal of Medicinal Chemistry, 2013 , vol. 70, p. 811 - 830
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; oxidation-Wittig reaction; 24 h;
参考文献
Runcie, Karen A.; Taylor, Richard J. K.
Chemical Communications, 2002 , # 9 p. 974 - 975