乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
tributyl-amine; 2-chloro-1-methyl-pyridinium iodide in toluene
T=110°C; 3 h;
参考文献
Kohl-Mines, Elisabeth; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1985 , vol. 68, p. 2244 - 2248
反应条件
benzoic acid in toluene
T=90°C; 18 h;
参考文献
BAYER HEALTHCARE AG
Patent: US2009/286882 A1, 2009 ;
Location in patent: Page/Page column 11-12 ;
反应条件
Benzoesaeure in benzene
2 h; Heating;
参考文献
Spitzner, Dietrich; Swoboda, Harald
Tetrahedron Letters, 1986 , vol. 27, # 11 p. 1281 - 1284
反应条件
potassium carbonate in ethyl acetate
4 h; Reflux;
参考文献
F. HOFFMANN-LA ROCHE AG; LIN, Xianfeng; QIU, Zongxing; TANG, Guozhi; WONG, Jason Christopher; ZHANG, Zhenshan
Patent: WO2012/98132 A1, 2012 ;
Location in patent: Page/Page column 72-74 ;
WO 2012/098132 A1
反应条件
zinc in toluene
2 h; Ambient temperature;
参考文献
Meshram; Reddy, Gondi Sudershan; Reddy, M. Muratidhar; Yadav
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 4107 - 4110
反应条件
in benzene
T=20°C; 1 h;
参考文献
Castaneda, Fernando; Aliaga, Christian; Bunton, Clifford A.; Garland, Maria Teresa; Baggio, Ricardo
Acta Crystallographica Section C: Crystal Structure Communications, 2005 , vol. 61, # 8 p. o496-o499
反应条件
in dichloromethane
T=25°C;
参考文献
Liu, Bin; Li, Kang-Nan; Luo, Shi-Wei; Huang, Jian-Zhou; Pang, Huan; Gong, Liu-Zhu
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3323 - 3326
反应条件
in N,N-dimethyl-formamide
0.1 h; microwave irradiation;
参考文献
Mohamed, Nadia Ragab; El-Saidi, Manal Mohamed Talaat; Ali, Yasser Mahmoud; Elnagdi, Mohamed Hilmy
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 6 p. 1333 - 1337
反应条件
in benzene
7 h; Heating;
参考文献
Oehme, G.; Pracejus, H.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 5 p. 798 - 808
反应条件
T=150 - 160°C; 2.5 h;
参考文献
Mali, R. S.; Yeola, Suresh N.
Synthesis, 1986 , # 9 p. 755 - 757
