乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
in benzene
Wittig Olefination; 8 h; Reflux;
参考文献
Radha Krishna, Palakodety; Prabhakar, Sunchu; Sravanthi, Chittela
Tetrahedron Letters, 2013 , vol. 54, # 7 p. 669 - 671
反应条件
N-chloro-succinimide; potassium carbonate
1.) CH2Cl2, -20 deg C, 20 min, 2.) CH2Cl2, RT, 24 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kayser, Margaret M.; Zhu, Jun; Hooper, Donald L.
Canadian Journal of Chemistry, 1997 , vol. 75, # 10 p. 1315 - 1321
参考文献
Ranade, A. C.; Mali, R. S.; Kurnawal, V. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 514 - 517
反应条件
N,N-diethylaniline
T=215°C; 6.5 h;
参考文献
Tanaka, Tomohiro; Kumamoto, Takuya; Ishikawa, Tsutomu
Tetrahedron Asymmetry, 2000 , vol. 11, # 23 p. 4633 - 4637
参考文献
Ranade, A. C.; Mali, R. S.; Kurnawal, V. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 514 - 517
反应条件
in ethanol; water
T=20°C;
参考文献
Richards, Elinor L; Murphy, Patrick J; Dinon, Francesca; Fratucello, Silvia; Brown, Paul M; Gelbrich, Thomas; Hursthouse, Michael B
Tetrahedron, 2001 , vol. 57, # 36 p. 7771 - 7784
反应条件
in dichloromethane
T=20°C; Wittig reaction; Inert atmosphereLarge scale reaction;
参考文献
Adam, Jean-Michel; Foricher, Joseph; Hanlon, Steven; Lohri, Bruno; Moine, Gerard; Schmid, Rudolf; Wirz, Beat; Zutter, Ulrich; Stahr, Helmut; Weber, Martin
Organic Process Research and Development, 2011 , vol. 15, # 3 p. 515 - 526
反应条件
in toluene
18 h; Heating / reflux; Product distribution / selectivity;
参考文献
ASTRAZENECA AB
Patent: WO2008/147314 A1, 2008 ;
Location in patent: Page/Page column 63 ;
WO 2008/147314 A1
反应条件
in benzene
4 h; Heating;
参考文献
Narasimhan, N. S.; Kusurkar, S. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 4 p. 345 - 348
反应条件
T=150°C; Yield given. Yields of byproduct given;
参考文献
Kuwahara; Sakuma
Agricultural and Biological Chemistry, 1982 , vol. 46, # 7 p. 1855 - 1860
