乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
参考文献
Mali, R. S.; Yeola, Suresh N.
Synthesis, 1986 , # 9 p. 755 - 757
反应条件
potassium carbonate in methanol; water; toluene
参考文献
Takeda Chemical Industries, Ltd.
Patent: US4590189 A1, 1986 ;
反应条件
in tetrahydrofuran
Yield given;
参考文献
Williams, Peter D.; LeGoff, Eugene
Tetrahedron Letters, 1985 , vol. 26, # 11 p. 1367 - 1370
反应条件
in dichloromethane
24 h; Reflux; Overall yield = 90 percent; Overall yield = 1.51 g;
参考文献
CANCER RESEARCH TECHNOLOGY LIMITED; GRIGG, Ronald Ernest; INMAN, Martyn; PACKHAM, Graham
Patent: WO2013/5049 A1, 2013 ;
Location in patent: Page/Page column 22 ;
反应条件
in dichloromethane
Ambient temperature; Title compound not separated from byproducts;
参考文献
Harris, Roger L. N.; McFadden, Helen G.
Australian Journal of Chemistry, 1984 , vol. 37, # 2 p. 417 - 424
反应条件
N,N-diethylaniline
Heating;
参考文献
Ray, Sutapa; Patra, Asit; Mal, Dipakranjan
Tetrahedron, 2008 , vol. 64, # 14 p. 3253 - 3267
反应条件
in tetrahydrofuran
T=65 - 75°C; 1 h;
参考文献
LG LIFE SCIENCES LTD.; KIM, Young Kwan; KIM, Myoung Yeol; PARK, Sang Yun; PARK, Ok Ku; ARTEMOV, Vasily; LEE, Sang Dae; JOO, Hyun Woo; CHOI, Eun Sil
Patent: WO2014/69963 A1, 2014 ;
Location in patent: Paragraph 1119-1121 ;
参考文献
Vertex Pharmaceuticals Incorporated
Patent: US2010/272681 A1, 2010 ;
反应条件
in tetrahydrofuran
T=25°C; 12 h;
参考文献
Williams, Peter D.; LeGoff, Eugene
Heterocycles, 1984 , vol. 22, # 2 p. 269 - 270
反应条件
in toluene
24 h; Heating;
参考文献
Joshi, U. K.; Kelkar, R. M.; Paradkar, M. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1151 - 1152
