乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
参考文献
Oehler, Elisabeth; Kang, Heun-Soo; Zbiral, Erich
Chemische Berichte, 1988 , vol. 121, p. 299 - 308
反应条件
in acetonitrile
T=190°C; 0.333333 h; microwave heating;
参考文献
Wu, Jinlong; Wu, Huafeng; Wei, Shaoyong; Dai, Wei-Min
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4401 - 4404
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=230°C; 0.333333 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Wu, Jinlong; Wu, Huafeng; Wei, Shaoyong; Dai, Wei-Min
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4401 - 4404
反应条件
1: With manganese(IV) oxide; benzoic acid in dichloromethane
T=20°C; 72 h;
2: With lithium aluminium tetrahydride in diethyl ether
T=0°C; 1 h;
3: With manganese(IV) oxide in dichloromethane
T=20°C; 78 h; Title compound not separated from byproducts;
参考文献
Petroski, Richard J.
Synthetic Communications, 2003 , vol. 33, # 18 p. 3233 - 3241
反应条件
barium permanganate in benzene
2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lee, Eun Young; Kim, Youngkwon; Lee, Jae Sung; Park, Jaiwook
European Journal of Organic Chemistry, 2009 , # 18 p. 2943 - 2946
反应条件
Dess-Martin periodane in dichloromethane
T=20°C; 20 h;
参考文献
Deng, Guisheng; Xu, Baihua; Liu, Chunyu
Tetrahedron, 2005 , vol. 61, # 24 p. 5818 - 5821
反应条件
pyridine-SO3 complex; triethylamine in dichloromethane; dimethyl sulfoxide
T=20°C; 2 h;
参考文献
Crisostomo, Fernando R. Pinacho; Carrillo, Romen; Martin, Tomas; Garcia-Tellado, Fernando; Martin, Victor S.
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 10099 - 10101
反应条件
1: benzylamine With palladium on activated charcoal
T=170°C; 3 h; Irradiationmicrowave;
2: ethyl (triphenylphosphoranylidene)acetate in water
T=20°C; Wittig reaction; 12 h;
参考文献
Chandrasekhar; Pavan Kumar Reddy; Nagesh; Raji Reddy
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1269 - 1271
反应条件
in dichloromethane
T=20°C;
参考文献
Chang, Meng-Yang; Lin, Chun-Yu; Sun, Pei-Pei
Journal of the Chinese Chemical Society, 2005 , vol. 52, # 5 p. 1061 - 1067
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; 4 h; other reactions cond., other reagents, other aldehydes; Product distribution;
参考文献
Dhavale, Dilip D.; Sindkhedkar, Milind D.; Mali, Raghao S.
Journal of Chemical Research, Synopses, 1995 , # 10 p. 414 - 415