乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
in benzene
Wittig olefination; 6 h; Heating;
参考文献
Kamal, Ahmed; Krishnaji, Tadiparthi; Reddy, P. Venkat
Tetrahedron Asymmetry, 2007 , vol. 18, # 15 p. 1775 - 1779
反应条件
manganese(IV) oxide in toluene
Oxidation; Wittig reaction; 6 h; Heating;
参考文献
Blackburn, Leonie; Wei, Xudong; Taylor, Richard J. K.
Chemical Communications, 1999 , # 14 p. 1337 - 1338
反应条件
in benzene
16 h; Heating;
参考文献
Pinhey, John T.; Stoermer, Martin J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 10 p. 2455 - 2460
反应条件
1: 3-phenylpropanol tert-butyldimethylsilyl ether With bismuth trifluoromethanesulphonate; water in acetonitrile
T=20°C; 1.5 h;
2: With 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; iodosylbenzene in acetonitrile
T=20°C; 2 h;
3: ethyl (triphenylphosphoranylidene)acetate in acetonitrile
T=0 - 20°C; 1 h; optical yield given as percent de;
参考文献
Barnych, Bogdan; Vatele, Jean-Michel
Synlett, 2011 , # 14 art. no. D10511ST, p. 2048 - 2052
反应条件
in N,N-dimethyl-formamide
16 h; Ambient temperature;
参考文献
Griengl; Hayden; Schwarz; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 2 p. 105 - 110
反应条件
oxygen in toluene
T=110°C; one-pot alcohol oxidation-Wittig reaction; 24 h;
参考文献
Lee, Eun Young; Kim, Youngkwon; Lee, Jae Sung; Park, Jaiwook
European Journal of Organic Chemistry, 2009 , # 18 p. 2943 - 2946
反应条件
1: in acetonitrile
2: With sodium hydroxide
参考文献
Yoo, Yeong Jae; Nam, Dong Hyuk; Jung, Seo Yun; Jang, Jae Wan; Kim, Hyoung Ja; Jin, Changbae; Pae, Ae Nim; Lee, Yong Sup
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 10 p. 2850 - 2854
反应条件
1: ethyl (triphenylphosphoranylidene)acetate; methyl halide in chloroform
RefluxInert atmosphere;
2: With triethylamine in dichloromethane
T=20°C; Inert atmosphere;
3: acetyl chloride in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Na, Risong; Jing, Chengfeng; Xu, Qihai; Jiang, Hui; Wu, Xi; Shi, Jiayan; Zhong, Jiangchun; Wang, Min; Benitez, Diego; Tkatchouk, Ekaterina; Goddard, William A.; Guo, Hongchao; Kwon, Ohyun
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13337 - 13348
反应条件
in benzene
4 h; Heating;
参考文献
Kovalev, B. G.; Dzhumakulov, T.; Abduvakhabov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 10 p. 1909 - 1912
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 10 p. 2116 - 2120
参考文献
Maillard; Langlois; Vo Van; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 4 p. 353 - 358
