乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
反应条件
benzoic acid in ethyl acetate
48 h; Heating;
参考文献
Kamel, Azza A.; Abdou, Wafaa M.
Synlett, 2007 , # 8 p. 1269 - 1273
反应条件
in 1,4-dioxane
72 h; Heating;
参考文献
Kamel, Azza A.; Abdou, Wafaa M.
Synlett, 2007 , # 8 p. 1269 - 1273
反应条件
1: in chloroform
Wittig reaction; 10 h; Reflux;
2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
10 h; Reflux;
参考文献
Chang, Meng-Yang; Lin, Chung-Han; Chen, Yeh-Long; Hsu, Ru-Ting; Chang, Ching-Yao
Tetrahedron Letters, 2010 , vol. 51, # 23 p. 3154 - 3158
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=230°C; Wittig reaction; 0.333333 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Wu, Jinlong; Li, Dan; Wu, Huafeng; Sun, Lijie; Dai, Wei-Min
Tetrahedron, 2006 , vol. 62, # 19 p. 4643 - 4650
反应条件
in benzene
T=45°C; 48 h;
参考文献
Doyle, Ian R.; Massy-Westropp, Ralph A.
Australian Journal of Chemistry, 1982 , vol. 35, # 9 p. 1903 - 1911
反应条件
1: in dichloromethane
Wittig Olefination;
2: With 2-pentafluorophenyl-6,17dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; triethylamine in tetrahydrofuran
Stetter 1,4-Dicarbonyl Synthesis; Inert atmosphere;
参考文献
Bromhead, Liam J.; Visser, Johan; McErlean, Christopher S. P.
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1516 - 1520
反应条件
N,N-dimethyl-aniline
T=200°C; 6 h;
参考文献
Mali, Raghao S.; Sandhu, Paramjeet Kaur; Manekar-Tilve, Anita
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 251 - 252
反应条件
N,N-dimethyl-aniline
Claisen rearrangement and Wittig reaction; 6 h; Heating;
参考文献
Mali, Raghao S.; Joshi, Priya P.; Sandhu, Paramjeet Kaur; Manekar-Tilve, Anita
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 371 - 376
参考文献
Bunce, Richard A.; Schilling III, Curtis L.
Tetrahedron, 1997 , vol. 53, # 28 p. 9477 - 9486
参考文献
Padwa, Albert; MacDonald, J. Gavin
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1225 - 1227