乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
1: T=20°C; Wittig olefination; 2 h;
2: Reflux;
参考文献
Pisani, Leonardo; Catto, Marco; Giangreco, Ilenia; Leonetti, Francesco; Nicolotti, Orazio; Stefanachi, Angela; Cellamare, Saverio; Carotti, Angelo
ChemMedChem, 2010 , vol. 5, # 9 p. 1616 - 1630
参考文献
Kalvoda,L.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 2034 - 2039
参考文献
D'Auria, Maurizio; Ferri, Tomaso
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8360 - 8364
反应条件
1: 35 g / benzene / 1.) 5 deg C, 10 min, 2.) 20 deg C, 15 min
2: sodium methanolate / methanol / 25 °C
View Scheme
参考文献
Cooke, Manning P.
Journal of Organic Chemistry, 1982 , vol. 47, # 25 p. 4963 - 4968
反应条件
zinc in toluene
3 h; Ambient temperature;
参考文献
Meshram; Reddy, Gondi Sudershan; Reddy, M. Muratidhar; Yadav
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 4107 - 4110
反应条件
in toluene
24 h; Reflux;
参考文献
Raghavan, Sadagopan; Sudheer Babu, Vaddela; Sridhar
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 557 - 565
参考文献
Jarolim; Sorm
Collection of Czechoslovak Chemical Communications, 1975 , vol. 40, # 4 p. 1059 - 1069
反应条件
in N,N-dimethyl-formamide
8 h; Heating;
参考文献
Abdou, Wafaa M.; Fahmy, Amin F. M.; Kamel, Azza A.
Heteroatom Chemistry, 2002 , vol. 13, # 4 p. 357 - 365
反应条件
in dichloromethane
T=20°C; Wittib reaction; 15 h;
参考文献
Nakamura, Masayuki; Mori, Yuichiro; Okuyama, Kennichi; Tanikawa, Kunihiro; Yasuda, Satoshi; Kanada, Kentaro; Kobayashi, Shu
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 19 p. 3362 - 3376
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=230°C; 0.333333 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Wu, Jinlong; Wu, Huafeng; Wei, Shaoyong; Dai, Wei-Min
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4401 - 4404
