乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
manganese(IV) oxide in dichloromethane T=20°C; Wittig olefination; 24 h;
参考文献
Phillips, David J.; Pillinger, Kathryn S.; Li, Wei; Taylor, Angela E.; Graham, Andrew E.
Chemical Communications, 2006 , # 21 p. 2280 - 2282
反应条件
zinc in toluene 2.5 h; Ambient temperature;
参考文献
Meshram; Reddy, Gondi Sudershan; Reddy, M. Muratidhar; Yadav
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 4107 - 4110
反应条件
in tetrahydrofuran 40 h; Ambient temperature;
参考文献
Wang; Huang
Synthetic Communications, 1994 , vol. 24, # 5 p. 689 - 693
反应条件
1: 2,2-dimethyl-5-hydroxymethyl-1,3-dioxane With oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78 - 0°C; Swern oxidation; 2: ethyl (triphenylphosphoranylidene)acetate in dichloromethane T=20°C; Wittig olefination; 2 h; Further stages.;
参考文献
Du, Yuguo; Liu, Jun; Linhardt, Robert J.
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3952 - 3954
反应条件
in methanol T=20°C; Wittig olefination;
参考文献
Du, Yuguo; Liu, Jun; Linhardt, Robert J.
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3952 - 3954
反应条件
Et2NC6H5 4 h; Heating;
参考文献
Maes, Dominick; Van Syngel, Kris; De Kimpe, Norbert
Heterocycles, 2008 , vol. 75, # 4 p. 1020 - 1021
反应条件
in dichloromethane T=0 - 20°C; 1.5 h; Large scale;
参考文献
PFIZER LIMITED; BAGAL, Sharanjeet Kaur; KEMP, Mark Ian; MILLER, Duncan Charles; MURATA, Yoshihisa
Patent: WO2013/61205 A2, 2013 ;
Location in patent: Page/Page column 67 ;
反应条件
1: in toluene T=20°C; Wittig reaction; 2: With triphenylphosphine; [MoO2Cl2(dmf)2] in toluene 24 h; Heating; Further stages.;
参考文献
Sanz, Roberto; Escribano, Jaime; Pedrosa, Maria R.; Aguado, Rafael; Arnaiz, Francisco J.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 4-5 p. 713 - 718
反应条件
sodium acetate in toluene 6 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 51, # 52 p. 6890 - 6892
反应条件
1: in toluene T=20°C; Wittig reaction; 2: With triphenylphosphine; [MoO2Cl2(dmf)2] in toluene 24 h; Heating; Further stages.;
参考文献
Sanz, Roberto; Escribano, Jaime; Pedrosa, Maria R.; Aguado, Rafael; Arnaiz, Francisco J.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 4-5 p. 713 - 718
