乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
参考文献
Latham, Elliot J.; Stanforth, Stephen P.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 14 p. 2059 - 2063
反应条件
selenium in toluene 3 h; Heating;
参考文献
Okuma, Kentaro; Sakata, Jun-ichi; Tachibana, Yuji; Honda, Takumi; Ohta, Hiroshi
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6649 - 6652
反应条件
selenium; n-butyllithium 1.) toluene; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Okuma, Kentaro; Kaneko, Isao; Ohta, Hiroshi; Yokomori, Yoshinobu
Heterocycles, 1990 , vol. 31, # 12 p. 2107 - 2110
反应条件
in xylene Wittig reaction; 13 h; Heating;
参考文献
Ranade, Anup A.; Joseph, Augustine R.; Kumbhar, Virendra B.; Paradkar, Madhusudan V.
Journal of Chemical Research, Miniprint, 2003 , # 8 p. 857 - 868
Title/Abstract Full Text Show Details
Ranade, Anup A.; Joseph, Augustine R.; Kumbhar, Virendra B.; Paradkar, Madhusudan V.
Journal of Chemical Research, Miniprint, 2003 , # 11 p. 1175 - 1184
反应条件
1: CH2Cl2 2: (i) Na, liq. NH3, DMF, (ii) H2O, benzene View Scheme
参考文献
Bestmann,H.-J. et al.
Chemische Berichte, 1973 , vol. 106, p. 2601 - 2609
反应条件
manganese(IV) oxide in toluene Oxidation; Wittig reaction; 4 h; Heating;
参考文献
Blackburn, Leonie; Wei, Xudong; Taylor, Richard J. K.
Chemical Communications, 1999 , # 14 p. 1337 - 1338
反应条件
barium permanganate in benzene 6 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shuto, Satoshi; Niizuma, Satoshi; Matsuda, Akira
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4489 - 4493
反应条件
in 1-methyl-pyrrolidin-2-one; toluene T=0°C; 72 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Hayashi, Yujiro; Samanta, Sampak; Itoh, Takahiko; Ishikawa, Hayato
Organic Letters, 2008 , vol. 10, # 24 p. 5581 - 5583
反应条件
T=20°C; Wittig reaction; 0.833333 h; Neat (no solvent)Air atmosphere;
参考文献
Orita, Akihiro; Okano, Junji; Uehara, Genta; Jiang, Lasheng; Otera, Junzo
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 8 p. 1617 - 1623
反应条件
manganese(IV) oxide; N-iodo-succinimide in dichloromethane 10 h; Sonication; optical yield given as percent destereoselective reaction;
参考文献
Karama, Usama
Synthetic Communications, 2010 , vol. 40, # 23 p. 3447 - 3451