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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
呋喃
合成路线
(共 939 条)
110-00-9
呋喃
→
反应条件
463-49-0
丙二烯
+
36998-21-7
+
50888-73-8
+
74-99-7
丙炔
反应条件
T=-263.2°C; Irradiation; Further byproducts given;
参考文献
Rendall, W. A.; Clement, A.; Torres, M.; Strausz, O. P.
Journal of the American Chemical Society, 1986 , vol. 108, # 7 p. 1691 - 1692
110-00-9
呋喃
→
反应条件
463-49-0
丙二烯
+
53268-92-1
+
36998-21-7
+
50888-73-8
+
74496-19-8
+
74-99-7
丙炔
反应条件
T=-263.2°C; Irradiationlow-temperature matrix photolysis; Product distribution;
参考文献
Rendall, W. A.; Clement, A.; Torres, M.; Strausz, O. P.
Journal of the American Chemical Society, 1986 , vol. 108, # 7 p. 1691 - 1692
110-00-9
呋喃
+
104-92-7
4-溴苯甲醚
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
1: furan With CdCl2*TMEDA; 2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; hexane T=20°C; 2 h; Inert atmosphere; 2: 1-bromo-4-methoxy-benzene With 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate in tetrahydrofuran; hexane T=60°C; 18 h; Inert atmosphere;
参考文献
L'Helgoual'ch, Jean-Martial; Bentabed-Ababsa, Ghenia; Chevallier, Floris; Yonehara, Mitsuhiro; Uchiyama, Masanobu; Derdour, Aicha; Mongin, Florence
Chemical Communications, 2008 , # 42 p. 5375 - 5377
110-00-9
呋喃
+
696-62-8
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
C52H44CoN4O4; potassium hydroxide; tert-butyl alcohol T=200°C; 1 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Qian, Ying Ying; Wong, Ka Lai; Zhang, Meng Wen; Kwok, Tsz Yiu; To, Ching Tat; Chan, Kin Shing
Tetrahedron Letters, 2012 , vol. 53, # 13 p. 1571 - 1575
110-00-9
呋喃
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
1: furan With n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; 0.75 h; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=0 - 20°C; 0.75 h; 3: 4-methoxyphenyl halide With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane 24 h; Reflux;
参考文献
Shinohara, Hiroyuki; Sonoda, Motohiro; Atobe, Shingo; Masuno, Haruna; Ogawa, Akiya
Tetrahedron Letters, 2011 , vol. 52, # 47 p. 6238 - 6241
110-00-9
呋喃
+
623-12-1
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
potassium phosphate; palladium diacetate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1-methyl-pyrrolidin-2-one T=15 - 100°C; 24.25 h; Inert atmosphere;
参考文献
Nadres, Enrico T.; Lazareva, Anna; Daugulis, Olafs
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 471 - 483
110-00-9
呋喃
+
104-94-9
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
tert.-butylnitrite; ascorbic acid powder in dimethyl sulfoxide; acetonitrile T=20°C; 12 h; Inert atmosphereGreen chemistry; regioselective reaction;
参考文献
Crisostomo, Fernando Pinacho; Martin, Tomas; Carrillo, Romen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 8 p. 2181 - 2185
Angew. Chem., 2014 , vol. 53, # 8 p. 2213 - 2217,5
110-00-9
呋喃
+
5720-07-0
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
Mn(OAc)3•2H2O in ethanol T=170°C; 0.166667 h; Microwave irradiation; regioselective reaction;
参考文献
Guchhait, Sankar K.; Kashyap, Maneesh; Saraf, Shuddham
Synthesis, 2010 , # 7 art. no. Z24009SS, p. 1166 - 1170
110-00-9
呋喃
+
459-64-3
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
18-crown-6 ether; potassium acetate
参考文献
Ellames, George J; Gibson, Jennifer S; Herbert, John M; McNeill, Alan H
Tetrahedron, 2001 , vol. 57, # 46 p. 9487 - 9497
110-00-9
呋喃
+
19501-58-7
→
反应条件
17113-31-4
(8CI)-2-(p-甲氧基苯基)-呋喃
反应条件
manganese triacetate Heating;
参考文献
Demir, Ayhan S.; Reis, Oemer; Emrullahoglu, Mustafa
Tetrahedron, 2002 , vol. 58, # 40 p. 8055 - 8058
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