反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium; ammonium chloride in hexane
under N2; to a soln. of furan and the amine in hexane is added sec-BuLidropwise at 0°C, after 1 h warmed to room temp., after 4 h cooled to 0°C, Me3SnCl in hexane is added dropwise, warmed to room temp.; after 24 h an aq. soln. of NH4Cl is added, the organic layer is washed,dried, the solvent is removed under reduced pressure, the residue is distd., elem. anal.;
参考文献
Seitz, David E.; Lee, Shi-Hung; Hanson, Robert N.; Bottaro, Jeffrey C.
Synthetic Communications, 1983 , vol. 13, # 2 p. 121 - 128
