反应条件
1: Li2CuCl4 / 1) THF -78 deg C, 2 hours 2) room temperature 15 h 2: 11.7 g / 5percent aq. HCl / acetone / 6 h / Ambient temperature 3: diisobutylaluminum hydride / diethyl ether / 1.5 h / -10 °C 4: 43 percent / pyridine / diethyl ether / 12 h / Ambient temperature; 1) 5 deg C, 1 h 2) room temperature 12 h 5: CuI, 2,2'-bipyridyl / 2 deg C, 2 h, THF View Scheme
参考文献
Odinokov, V. N.; Galeeva, R. I.; Kargapol'tseva, T. A.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 666 - 668
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 735 - 738
