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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
溴代正戊烷
合成路线
（共 639 条）
→
反应条件
111-84-2
壬烷
+
538-68-1
戊基苯
反应条件
Ni catalyst in tetrahydrofuran
参考文献
Pekel, Oezgen Oemuer; Erdik, Ender
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7087 - 7090
693-03-8
溴丁基-镁
+
629-04-9
1-溴代庚烷
+
110-53-2
溴代正戊烷
→
反应条件
111-84-2
壬烷
+
1120-21-4
十一烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 1-n-heptylbromide; n-bromopentane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Erdik, Ender; Oezkan, Duygu
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
507-19-7
溴代叔丁烷
+
110-53-2
溴代正戊烷
→
反应条件
590-73-8
2,2-二甲基己烷
+
111-84-2
壬烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With n-butyl-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 1-bromo-1,1-dimethylethane; n-bromopentane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Erdik, Ender; Oezkan, Duygu
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
78-77-3
溴代异丁烷
+
110-53-2
溴代正戊烷
→
反应条件
592-27-8
2-甲基庚烷
+
111-84-2
壬烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 2-methyl-1-bromopropane; n-bromopentane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Erdik, Ender; Oezkan, Duygu
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
110-53-2
溴代正戊烷
+
111-83-1
溴辛烷
→
反应条件
111-84-2
壬烷
+
112-40-3
正十二烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-bromopentane; 1-bromo-octane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Erdik, Ender; Oezkan, Duygu
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
110-53-2
溴代正戊烷
+
100-39-0
溴化苄
→
反应条件
111-84-2
壬烷
+
538-68-1
戊基苯
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-bromopentane; benzyl bromide in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Erdik, Ender; Oezkan, Duygu
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
110-53-2
溴代正戊烷
+
103-63-9
(2-溴乙基)苯
→
反应条件
111-84-2
壬烷
+
1077-16-3
己基苯
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With n-butyl-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-bromopentane; 2-(phenyl)ethyl bromide in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Erdik, Ender; Oezkan, Duygu
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 12 p. 1148 - 1154
110-53-2
溴代正戊烷
→
反应条件
872-10-6
正戊基硫醚
反应条件
disulfur-ion; lt;Pgt;-(CH2)3-+PBu3 in water T=110°C; 1.5 h;
参考文献
Chiles, Margaret Shea; Jackson, Donald D.; Reeves, Perry C.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2915 - 2918
110-53-2
溴代正戊烷
→
反应条件
872-10-6
正戊基硫醚
+
112-51-6
二戊基二硫醚
反应条件
H4Mo2S12(2-)*2H(1+)*2H3N in benzene T=90°C; acetonitrile; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Harpp, David N.; MacDonald, J. Gavin
Tetrahedron Letters, 1984 , vol. 25, # 7 p. 703 - 706
110-53-2
溴代正戊烷
→
反应条件
124-18-5
癸烷
反应条件
sodium
参考文献
Stratford
Annales de l'Office National des Combustibles Liquides (France), 1929 , vol. 4, p. 321
Chem. Zentralbl., 1929 , vol. 100, # II p. 1286
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