1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C;
2: n-bromopentane With tetra-(n-butyl)ammonium iodide in tetrahydrofuran
16 h; Heating;
1: 4-Methylpyridine With n-butyllithium in tetrahydrofuran
T=-78 - 45°C; 2 h;
2: n-bromopentane in tetrahydrofuran
T=-78 - 20°C;
3: With water in tetrahydrofuran
参考文献
THE UNIVERSITY OF SYDNEY
Patent: WO2007/128059 A1, 2007 ;
Location in patent: Page/Page column 23-24 ;
WO 2007/128059 A1
