ammonium nitrate in ethanol
144 h; Ambient temperature;
参考文献
Rulev, A. Yu.; Mokov, A. S.; Krivdin, L. B.; Keiko, N. A.; Voronkov, M. G.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1465 - 1469
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1634 - 1638
Aggarwal, Varinder K.; Alonso, Emma; Hynd, George; Lydon, Kevin M.; Palmer, Matthew J.; Porcelloni, Marina; Studley, John R.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 8 p. 1430 - 1433
sodium methylsulfinylmethanide in tetrahydrofuran; dimethyl sulfoxide
T=5°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiike; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 9 p. 2229 - 2230
(S)-5,5',6,6',7,7',8,8'-octahydro-3,3'-bis(4-morpholinylmethyl)-[1,1'-binaphthalene]-2,2'-diol
T=20°C; 12 h; Title compound not separated from byproducts;
参考文献
Qin, Ying-Chuan; Pu, Lin
Angewandte Chemie - International Edition, 2006 , vol. 45, # 2 p. 273 - 277
1: phenyl-magnesium bromide With titanium(IV) isopropylate in dichloromethane
T=-78°C; 0.166667 h; Inert atmosphere;
2: pentanal With 3-(3,5-diphenylphenyl)-H8-BINOL in diethyl ether; dichloromethane
T=0°C; 3 h; Inert atmosphere;
3: With hydrogenchloride; water in diethyl ether; dichloromethane
T=0°C; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Muramatsu, Yusuke; Harada, Toshiro
Chemistry - A European Journal, 2008 , vol. 14, # 34 p. 10560 - 10563
