Silveira, Claudio C.; Mendes, Samuel R.; Ziembowicz, Francieli I.; Lenardao, Eder J.; Perin, Gelson
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 2 p. 371 - 374
1.1: MeLi / tetrahydrofuran; diethyl ether / 0.25 h / -10 °C
1.2: 90 percent / tetrahydrofuran; diethyl ether / 2 h / -40 - 20 °C
2.1: 89 percent / TBAF / tetrahydrofuran
3.1: 85 percent / H2; TEA / Pd-BaSO4 / 0.75 h / 760 Torr
View Scheme
参考文献
Schwartz, Brett D.; McErlean, Christopher S. P.; Fletcher, Mary T.; Mazomenos, Basilis E.; Konstantopoulou, Maria A.; Kitching, William; De Voss, James J.
Organic Letters, 2005 , vol. 7, # 6 p. 1173 - 1176
sodium methylsulfinylmethanide in tetrahydrofuran; dimethyl sulfoxide
T=5°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiike; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 9 p. 2229 - 2230
