N,N'-二甲基乙二胺合成路线 （共 190 条）
反应条件
in tetrahydrofuran
Ambient temperature;
参考文献
Xu, Daqiang; Mattner, Paul G.; Prasad, Kapa; Repic, Oljan; Blacklock, Thomas J.
Tetrahedron Letters, 1996 , vol. 37, # 30 p. 5301 - 5304
反应条件
in tetrahydrofuran
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Xu, Daqiang; Prasad, Kapa; Repic, Oljan; Blacklock, Thomas J.
Tetrahedron Letters, 1995 , vol. 36, # 41 p. 7357 - 7360
反应条件
in water
T=95°C; 0.25 h;
参考文献
Ge, Shaozhong; Bambirra, Sergio; Meetsma, Auke; Hessen, Bart
Chemical Communications, 2006 , # 31 p. 3320 - 3322
反应条件
triethylamine in benzene
0.75 h;
参考文献
Nunez, Andres; Berroteran, Dyanna; Nunez, Oswaldo
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2283 - 2289
反应条件
potassium phosphate; CuI in N-methyl-acetamide
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
T=20°C; 0.5 h; Cooling with acetone-dry ice;
参考文献
MIRUS CORPORATION
Patent: WO2003/99225 A2, 2003 ;
Location in patent: Page 23-24 ;
参考文献
Wrackmeyer,B.; Noeth,H.
Chemische Berichte, 1977 , vol. 110, p. 1086 - 1094
反应条件
triethylamine in diethyl ether
参考文献
Nakanishi,A. et al.
Journal of the American Chemical Society, 1978 , vol. 100, p. 6398 - 6402
反应条件
in diethyl ether
T=20°C;
参考文献
Fu, Nanyan; Allen, Annette D.; Kobayashi, Shinjiro; Tidwell, Thomas T.; Vukovic, Sinisa; Arumugam, Selvananthan; Popik, Vladimir V.; Mishima, Masaaki
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 1951 - 1956
反应条件
phosphorus tribromide; triethylamine in diethyl ether
参考文献
Becker, W.; Schiebel, H. M.; Schmutzler, R.
Chemische Berichte, 1992 , vol. 125, # 4 p. 793 - 800
