N,N'-二甲基乙二胺合成路线 (共 190 条)
反应条件
iodine in tetrahydrofuran
byproducts: NaI; boiling under nitrogene;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
参考文献
Costantino, Gabriele; Marinozzi, Maura; Camaioni, Emidio; Natalini, Benedetto; Sarichelou, Iran; Micheli, Fabrizio; Cavanni, Paolo; Faedo, Stefania; Noe, Christian; Moroni, Flavio; Pellicciari, Roberto
Farmaco, 2004 , vol. 59, # 2 p. 93 - 99
反应条件
in N,N-dimethyl-formamide
T=20°C;
参考文献
Hassan, Alaa A.; Mourad, Aboul-Fetouh E.; El-Shaieb, Kamal M.; Abou-Zied, Ashraf H.; Doepp, Dietrich
Heteroatom Chemistry, 2003 , vol. 14, # 6 p. 535 - 541
反应条件
in benzene
20 h; Heating;
参考文献
Robbe; Fernandez; Dubief; et al.
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 3 p. 235 - 243
反应条件
pyridine; thionyl chloride
1) CH2Cl2, 0 deg C to r.t. 1 h, 2) 5 min; Yield given. Multistep reaction;
参考文献
Eynde, J.-J. Vanden; Mayence, A.; Maquestiau, A.; Anders, E.
Bulletin des Societes Chimiques Belges, 1992 , vol. 101, # 3 p. 233 - 236
参考文献
Savignac,P. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1978 , vol. 287, p. 35 - 38
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947