N,N'-二甲基乙二胺合成路线 （共 190 条）
反应条件
in dichloromethane 2 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2006/23400 A2, 2006 ;
Location in patent: Page/Page column 150-151 ;
反应条件
in N,N-dimethyl-formamide 7 h; Heating;
参考文献
Julia, Luis; Rius, Jordi; Suschitzky, Hans
Heterocycles, 1992 , vol. 34, # 8 p. 1539 - 1545
反应条件
sodium carbonate; triethylamine in methanol
参考文献
Sterling Drug Inc.
Patent: US5068234 A1, 1991 ;
反应条件
triethylamine in benzene 3 h; Heating;
参考文献
Manetti, Dina; Bartolini, Alessandro; Borea, Pier Andrea; Bellucci, Cristina; Dei, Silvia; Ghelardini, Carla; Gualtieri, Fulvio; Romanelli, Maria Novella; Scapecchi, Serena; Teodori, Elisabetta; Varani, Katia
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 3 p. 457 - 465
反应条件
tetraphosphorus decasulfide; triphenyl antimony oxide in benzene T=100°C; P=36752.9 Torr;
参考文献
Journal of Organic Chemistry, , vol. 57, # 28 p. 7339 - 7342
参考文献
Gol'din,G.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1978 , vol. 48, # 1 p. 129 - 131,109 - 111
反应条件
n-butyllithium in diethyl ether; hexane T=-78 - 20°C;
参考文献
Oka, Natsuhisa; Shimizu, Mamoru; Saigo, Kazuhiko; Wada, Takeshi
Tetrahedron, 2006 , vol. 62, # 15 p. 3667 - 3673
反应条件
in neat (no solvent) byproducts: dimethylamine; 120°C, 5h;
参考文献
Brown,M.P. et al.
Journal of the Chemical Society, 1962 , p. 4648 - 4652
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Gmelin Handbook: B: B-Verb.1, 2.5.2.2, page 130 - 132
反应条件
N(C2H5)3 in hexane byproducts: ((C2H5)3NH)Cl; under N2, addn. of both amines in hexane to a stirred hexane soln. of B-compd. at -30°C, refluxed for 17 h; centrifugation, hexane evapd., fractional distn.;
参考文献
Loderer, Dirk; Noeth, Heinrich; Pommerening, Hans; Rattay, Wilfried; Schick, Hannes
Chemische Berichte, 1994 , vol. 127, # 9 p. 1605 - 1612
反应条件
byproducts: ClNH2(CH3)C2H4(CH3)NH2Cl; molar ratio of B2Cl4 and amine = 1:4;
参考文献
Welch; Shore
Inorganic Chemistry, 1968 , vol. 7, p. 225,226, 227, 230
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Gmelin Handbook: B: B-Verb.1, 2.5.2.2, page 130 - 132
