N,N'-二甲基乙二胺合成路线 (共 190 条)
反应条件
transamination, boiling the reactants under nitrogene in inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling of the educts in inert atmosphere, distn. of the dimethylamine during the reaction; distn.;
参考文献
Fritz, P. W.; Niedenzu, K.; Dawson, J. W.
Inorganic Chemistry, 1964 , vol. 3, p. 626 - 626
反应条件
in diethyl ether T=20°C;
参考文献
GEORGIA TECH RESEARCH CORPORATION
Patent: WO2005/123754 A2, 2005 ;
Location in patent: Page/Page column 45-46; Sheet 19 ;
反应条件
in diethyl ether T=25°C; 12 h;
参考文献
Takada, Yoshiaki; Nomura, Kenichi; Matsubara, Seijiro
Organic Letters, 2010 , vol. 12, # 22 p. 5204 - 5205
反应条件
N,O-bis-(trimethylsilyl)-acetamide; CuI; KF in toluene
参考文献
Idemitsu Kosan Co., Ltd.
Patent: US2007/29927 A1, 2007 ;
反应条件
in toluene 24 h; Heating;
参考文献
Wang, Mei-Xiang; Liang, Jing-Mei; Huang, Zhi-Tang
Journal of Chemical Research, Miniprint, 1994 , # 5 p. 1001 - 1019
参考文献
IBC Advanced Technologies, Inc.
Patent: US2003/50458 A1, 2003 ;
参考文献
Kutter; Machleidt; Reuter; Sauter; Wildfeuer
Arzneimittel-Forschung, 1972 , vol. 22, # 6 p. 1045 - 1054
反应条件
triethylamine in dichloromethane T=30°C; 30 h;
参考文献
Newkome, George R.; Kawato, Toshio
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 629 - 632