N,N'-二甲基乙二胺合成路线 (共 190 条)
反应条件
sodium hydrogencarbonate in ethanol Heating;
参考文献
Bolos, Jordi; Gubert, Santiago; Anglada, Lluis; Planas, Josep M.; Burgarolas, Carme; Castello, Josep M.; Sacristan, Aurelio; Ortiz, Jose A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 15 p. 2962 - 2970
反应条件
sodium carbonate; triethylamine in methanol
参考文献
Sterling Drug Inc.
Patent: US5068234 A1, 1991 ;
反应条件
potassium carbonate in butan-1-ol 6 h; Heating; Title compound not separated from byproducts;
参考文献
Tomashevskii; Sokolov; Potekhin
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 4 p. 583 - 588
反应条件
potassium carbonate in butan-1-ol 6 h; Heating; Title compound not separated from byproducts;
参考文献
Tomashevskii; Sokolov; Potekhin
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 4 p. 583 - 588
反应条件
potassium carbonate in butan-1-ol 6 h; Heating; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Tomashevskii; Sokolov; Potekhin
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 4 p. 583 - 588
反应条件
triethylamine in benzene 1.5 h; Ambient temperature;
参考文献
Hanessian, Stephen; Bennani, Youssef L.; Leblanc, Yves
Heterocycles, 1993 , vol. 35, # 2 p. 1411 - 1424
反应条件
hydrogenchloride in water treatment of Pt-complex with ligand in aqueous soln. acidified with HCl; filtn., dissolving in dmf, reprecipitating by addn. of water and HCl, left to stand overnight;
参考文献
Peloso, Arnaldo
Polyhedron, 1992 , vol. 11, p. 2187 - 2194
反应条件
potassium hydroxide 1.) ethanol, 70 deg C, 10 h, 2.) ethanol, 35 deg C - 40 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Ismiev, A. I.; Farzaliev, V. M.; Allakhverdiev, M. A.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 6.2 p. 1196
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 6 p. 1366 - 1367
反应条件
potassium hydroxide in methanol Inert atmosphereReflux;
参考文献
Pandiyan, Thangarasu; Guadalupe, Hernandez J.; Cruz, Julian; Bernes, Sylvain; Ugalde-Salvdivar, Victor M.; Gonzalez, Ignacio
European Journal of Inorganic Chemistry, 2008 , # 21 p. 3274 - 3285
反应条件
sodium hydroxide in dichloromethane; water T=20°C; 60 h;
参考文献
Iturrospe, Amaia; Artetxe, Benat; Reinoso, Santiago; San Felices, Leire; Vitoria, Pablo; Lezama, Luis; Gutierrez-Zorrilla, Juan M.
Inorganic Chemistry, 2013 , vol. 52, # 6 p. 3084 - 3093