Hg in ethylene glycol dimethyl ether Sonication; (N2), DME added to excess of Sm metal, Sn complex and 1-2 drops of Hg, sonicated at room temp. for 5 d; filtered, concd., crystd. at -20°C, washed (hexane), dried (vac.), elem. anal.;
参考文献
Beaini, Samar; Deacon, Glen B.; Hilder, Matthias; Junk, Peter C.; Turner, David R.
European Journal of Inorganic Chemistry, 2006 , # 17 p. 3434 - 3441
Hg in ethylene glycol dimethyl ether Sonication; (N2), DME added to excess of Yb metal, Sn complex and 1-2 drops of Hg, sonicated at room temp. for 5 d; filtered, concd., crystd. at -20°C, washed (hexane), dried (vac.), elem. anal.;
参考文献
Beaini, Samar; Deacon, Glen B.; Hilder, Matthias; Junk, Peter C.; Turner, David R.
European Journal of Inorganic Chemistry, 2006 , # 17 p. 3434 - 3441
Hg in ethylene glycol dimethyl ether (N2), DME added to excess of La metal, Sn complex and 1-2 drops of Hg, stirred at room temp. for 5 d; filtered, concd., crystd. at -20°C, washed (hexane), dried (vac.), elem. anal.;
参考文献
Beaini, Samar; Deacon, Glen B.; Hilder, Matthias; Junk, Peter C.; Turner, David R.
European Journal of Inorganic Chemistry, 2006 , # 17 p. 3434 - 3441
Hg in ethylene glycol dimethyl ether (N2), DME added to excess of Nd metal, Sn complex and 1-2 drops of Hg, stirred at room temp. for 5 d; filtered, concd., crystd. at -20°C, washed (hexane), dried (vac.), elem. anal.;
参考文献
Beaini, Samar; Deacon, Glen B.; Hilder, Matthias; Junk, Peter C.; Turner, David R.
European Journal of Inorganic Chemistry, 2006 , # 17 p. 3434 - 3441
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反应条件
Hg in ethylene glycol dimethyl ether (N2), DME added to excess of Sm metal, Sn complex and 1-2 drops of Hg, stirred at room temp. for 3 d; filtered, concd., crystd. at -20°C, washed (hexane), dried (vac.), elem. anal.;
参考文献
Beaini, Samar; Deacon, Glen B.; Hilder, Matthias; Junk, Peter C.; Turner, David R.
European Journal of Inorganic Chemistry, 2006 , # 17 p. 3434 - 3441
