air in tetrahydrofuran
byproducts: cyclohexane; N2-atmosphere; treatment of B2H6 with olefin, addn. of MeSH (stirring), injecting small amt. of air (in two steps during 2 h), stirring for 12 h; evapn. of volatiles (reduced pressure), fractional distn. (reduced pressure);
参考文献
Pelter,A. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 2087 - 2090
(i) B2H6, Et2O, (ii) /BRN= 906737/; Multistep reaction;
参考文献
Mikhailov,B.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 579 - 582
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , p. 646 - 651
Levas
Annales de Chimie (Cachan, France), 1948 , vol. <12> 3, p. 145,191
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 223, p. 901,903 Anm.
