in further solvent(s) dissolving Ni(ClO4)2*6H2O in 2.2-dimethoxy-propane, drying under stirring within 3 h, addn. of pyridine;; pptn., filtering off, washing several times with ether, drying, suspending in ether, filtering off, washing and drying for 12 h at 25°C in vac.;;
参考文献
Brown, D. H.; Nuttall, R. H.; McAvoy, J.; Sharp, D. W. A.
Journal of the Chemical Society [Section] A: Inorganic, Physical, Theoretical, 1966 , p. 892 - 896
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Gmelin Handbook: Ni: MVol.C1, 108, page 251 - 253
1: water; ethanol 2: neat (no solvent) View Scheme
参考文献
Bull, W. E.; Moore, L. E.
Journal of Inorganic and Nuclear Chemistry, 1965 , vol. 27, p. 1341 - 1350
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Gmelin Handbook: Ni: MVol.C1, 108, page 251 - 253
in methanol soln. of Mn(II) chloride in methanol added to soln. of pyridine in methanol in 1:2 mol. ratio with continuous stirring for 30 min; react. mixt. left overnight at room temp.; ppt. isolated by filtration; washed in CH3OH; dried in vacuo;
参考文献
Siddiqi; Nami, Shahab A. A.; Lutfullah; Chebude, Yonas
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2005 , vol. 35, # 6 p. 445 - 451
in water to an aq. soln. of Co(NO3)2*6H2O and pyridine slowly added an aq. soln. of NaNCS; pink precipitate filtered off and washed with ethanol-pyridine (9:1); drying in vacuo;
dipotassium hydrogenphosphate; sodium dithionite in water T=65°C; P=2250.2 - 3750.3 Torr; 2 h;
参考文献
Tordeux, Marc; Langlois, Bernard; Wakselman, Claude
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2293 - 2299
