反应条件
in sodium hydroxide; diethyl ether; benzene
vigorous stirring (2 h, room temp.), addn. of ether, stirring (10 min); sepn. of org. layer, extn. of aq. layer (ether), drying (Na2SO4), removal of solvent (vac.), addn. of hexane, sepn. of org. byproduct, removal of hexane (vac.),sepn. of cis/trans (total yield 86.8percent) on crystn. (hexane); elem. anal.;
参考文献
Boev, V. I.; Dombrovskii, A. V.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 103 - 106
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 121 - 125
