1,2-二碘-4,5-二甲氧基苯合成路线 （共 14 条）
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate; zinc(II) chloride in acetic acid 4 h; Ambient temperature;
参考文献
Lacour, Jerome; Monchaud, David; Bernardinelli, Gerald; Favarger, France
Organic Letters, 2001 , vol. 3, # 9 p. 1407 - 1410
反应条件
[bis(acetoxy)iodo]benzene; lithium iodide in 1,1,1,3,3,3-hexafluoroisopropanol T=20°C; Hunsdiecker type reaction;
参考文献
Hamamoto, Hiromi; Hattori, Sho; Takemaru, Kaori; Miki, Yasuyoshi
Synlett, 2011 , # 11 p. 1563 - 1566
反应条件
sulfuric acid; iodine in acetonitrile T=0°C; 0.5 h; ElectrolysisFlow reactor; regioselective reaction;
参考文献
Organic Process Research and Development, , vol. 12, # 6 p. 1130 - 1136
反应条件
iodine; isopentyl nitrite in 1,4-dioxane; chloroform-d1 Heating;
参考文献
Perry, Robert J.; Turner, S. Richard
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6573 - 6579
反应条件
ethanol; sulfuric acid; dihydrogen peroxide; iodine
参考文献
Austral. J. scient. Res., , vol. <A> 2, p. 595,599
反应条件
n-butyllithium in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Hsu, Shih-Fan; Ko, Chih-Wei; Wu, Yao-Ting
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1756 - 1762
反应条件
1: 43 percent / BBr3 / CH2Cl2 / 1 h / 20 °C 2: 82 percent / Pd(PPh3)2Cl2; CuI; triethylamine / 5 h / 20 °C 3: 80 percent / aq. KOH / methanol / 1 h / 20 °C 4: 68 percent / triethylamine; Pd(PPh3)2Cl2 / dimethylformamide / 4 h / 70 °C View Scheme
参考文献
Peng, Zhonghua; Pan, Yongchun; Xu, Bubin; Zhang, Jianheng
Journal of the American Chemical Society, 2000 , vol. 122, # 28 p. 6619 - 6623
反应条件
1: 81 percent / B-Br-9-BBN / CH2Cl2 / 72 h / Heating 2: Pd(PPh3)2Cl2; Et3N / dimethylformamide 3: TBAF / tetrahydrofuran View Scheme
参考文献
Peng, Zhonghua; Pan, Yongchun; Xu, Bubin; Zhang, Jianheng
Journal of the American Chemical Society, 2000 , vol. 122, # 28 p. 6619 - 6623
反应条件
1: glacial acetic acid; nitric acid 2: nitric acid View Scheme
参考文献
Robinson
Journal of the Chemical Society, 1916 , vol. 109, p. 1087
反应条件
1: NEt3 / Pd(PPh3)2Cl2; CuI / dimethylformamide 2: Bu4NF / tetrahydrofuran View Scheme
参考文献
Juricek, Michal; Stout, Kathleen; Kouwer, Paul H.J.; Rowan, Alan E.
Journal of Porphyrins and Phthalocyanines, 2011 , vol. 15, # 9-10 p. 898 - 907
