1,2-二碘-4,5-二甲氧基苯合成路线 (共 14 条)
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; triethylamine 1) RT, 2) MeOH, RT; Yield given. Multistep reaction;
参考文献
Grissom, Janet Wisniewski; Gunawardena, Gamini U.
Tetrahedron Letters, 1995 , vol. 36, # 28 p. 4951 - 4954
反应条件
1: With boron tribromide in dichloromethane T=0°C; 4 h; Inert atmosphere; 2: With water
参考文献
Fisher, Thomas J.; Canete, Socrates Jose P.; Lai, Rebecca Y.; Dussault, Patrick H.
European Journal of Organic Chemistry, 2013 , # 16 p. 3263 - 3270
反应条件
piperidine; bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide; copper(l) iodide in ethanol; dichloromethane
T=20°C; 12 h;
参考文献
Shotwell, Sandra; Windscheif, Paul M.; Smith, Mark D.; Bunz, Uwe H. F.
Organic Letters, 2004 , vol. 6, # 23 p. 4151 - 4154
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; ammonia in tetrahydrofuran; water
T=20°C; Sonogashira coupling; 24 h; Inert atmosphere;
参考文献
Jung, Miso; Suzaki, Yuji; Saito, Takashi; Shimada, Kyoichi; Osakada, Kohtaro
Polyhedron, 2012 , vol. 40, # 1 p. 168 - 174