反应条件
1: 73 percent / t-butylhydroperoxide / VO(acac)2 / toluene
2: 60 percent / tetrabutylammonium iodide
3: 30 percent / KHF2 / ethane-1,2-diol / 160 °C
4: 56 percent / ethyldiisopropylamine / CH2Cl2
5: hydrogen, H(1+) / Pd/C / ethyl acetate
6: triethylamine, 4-dimethylaminopyridine
7: 18 percent / potassium carbonate / dimethylsulfoxide / 80 °C
8: 1 M HCl / Heating
View Scheme
参考文献
Borthwick; Butt; Biggadike; Exall; Roberts; Youds; Kirk; Booth; Cameron; Cox; Marr; Shill
Journal of the Chemical Society - Series Chemical Communications, 1988 , # 10 p. 656 - 658