(8R,9S,13S,14S,17S)-17-(6-羟基己基氨基)-13-甲基-6,7,8,9,11,12,14,15,16,17-十氢环戊烯并[a]菲-3-醇合成路线 （共 3 条）
→
110346-23-1(8R,9S,13S,14S,17S)-17-(6-羟基己基氨基)-13-甲基-6,7,8,9,11,12,14,15,16,17-十氢环戊烯并[a]菲-3-醇
反应条件
sodium tetrahydroborate in ethanol 1) 3 h, 2) r.t., overnight; Yield given;
参考文献
Steroids, , vol. 46, # 4-5 p. 889 - 902
→
110346-23-1(8R,9S,13S,14S,17S)-17-(6-羟基己基氨基)-13-甲基-6,7,8,9,11,12,14,15,16,17-十氢环戊烯并[a]菲-3-醇
反应条件
1: 73 percent / 80 °C / overnight 2: NaBH4 / ethanol / 1) 3 h, 2) r.t., overnight View Scheme
参考文献
Steroids, , vol. 46, # 4-5 p. 889 - 902
→
110346-23-1(8R,9S,13S,14S,17S)-17-(6-羟基己基氨基)-13-甲基-6,7,8,9,11,12,14,15,16,17-十氢环戊烯并[a]菲-3-醇
反应条件
1: 73 percent / 80 °C / overnight 2: NaBH4 / ethanol / 1) 3 h, 2) r.t., overnight View Scheme
参考文献
Steroids, , vol. 46, # 4-5 p. 889 - 902
