反应条件
in toluene
byproducts: trimethylamine; Ar atmosphere, stirring (80-90°C, 3.5 h); solvent removal (14 Torr), B-products (1:1 mixt., not separated) isolated by distn. (25-30, 0.001 Torr), identified ny MS, (1)H- and (11)B-NMR; byproducts identified by MS and (31)P-NMR;
参考文献
Koester, Roland; Seidel, Guenter; Mueller, Gerhard; Boese, Roland; Wrackmeyer, Bernd
Chemische Berichte, 1988 , vol. 121, p. 1381 - 1392
