反应条件
1: 82 percent / CHCl3 / 22 h / 22 °C
2: 99 percent / H2 / 10percent Pd/C / methanol / 3102.9 Torr
3: 56 percent / m-CPBA / CH2Cl2 / 0.28 h / Heating
4: 86 percent / KF / acetonitrile / 24 h / 22 °C
5: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C
6: 84 percent / zinc dust, acetic acid / tetrahydrofuran / 0.25 h / 45 °C
7: 81 percent / cerium(IV) ammonium nitrate, HNO3 / ethanol / 0.25 h / -42 °C
8: 80 percent / L-selectride / tetrahydrofuran / 2 h / -78 °C
9: pyridine / 1 h / 0 °C
10: 100 percent / sodium azide, ammonium chloride / dimethylformamide / 16 h / 22 °C
11: 4 N HCl / dioxane / 96 h / 22 °C
12: 554 mg / sodium acetate / 6.5 h / 50 °C
13: 59 percent / SnCl4 / CH2Cl2; acetonitrile / 16 h / 22 °C
14: 88 percent / potassium carbonate, acetic acid / methanol / 0.75 h / 22 °C
15: 91 percent / H2 / palladium hydroxide on carbon / methanol / 44 h / 3102.9 Torr
16: trifluoroacetic acid/water (9/1) / 1 h / 22 °C
17: 49 percent / liquid ammonia, sodium / -78 °C
View Scheme
参考文献
Maguire, Martin P.; Feldman, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 948 - 955
