4-氟四氢-2H-吡喃-4-甲醛合成路线 （共 2 条）
反应条件
1: With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine in dichloromethane T=0 - 20°C; 2 h; 2: With N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in dichloromethane T=0 - 20°C; 3 h;
参考文献
NOVARTIS AG; BARSANTI, Paul A.; HU, Cheng; JIN, Xianming; NG, Simon C.; PFISTER, Keith B.; SENDZIK, Martin; SUTTON, James
Patent: WO2012/101063 A1, 2012 ;
Location in patent: Page/Page column 115-116 ;
WO 2012/101063 A1
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in dichloromethane T=0 - 20°C; 3 h;
参考文献
NOVARTIS AG; ANTONIOS-MCCREA, William R.; BARSANTI, Paul A.; HU, Cheng; JIN, Xianming; LIN, Xiaodong; MARTIN, Eric J.; PAN, Yue; PFISTER, Keith B.; RENHOWE, Paul A.; SENDZIK, Martin; SUTTON, James; WAN, Lifeng
Patent: WO2012/101066 A1, 2012 ;
Location in patent: Page/Page column 101; 169 ;
WO 2012/101066 A1
