hydrogen; palladium on activated charcoal in acetic acid 1 h; Ambient temperature;

Multi-step reaction with 8 steps 1: 92 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature2: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature3: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux4: 58 percent / 1 h / 200 °C5: 94 percent / H2 / Pt-oxide / acetic acid / 1 h6: 62 percent / K2CO3 / 16 h / Ambient temperature7: 6 h / 60 °C8: 15 percent HCl / 1) 16 h, r.t.; 2) 30 min, 60 deg C  

Multi-step reaction with 7 steps 1: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature2: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux3: 58 percent / 1 h / 200 °C4: 94 percent / H2 / Pt-oxide / acetic acid / 1 h5: 62 percent / K2CO3 / 16 h / Ambient temperature6: 6 h / 60 °C7: 15 percent HCl / 1) 16 h, r.t.; 2) 30 min, 60 deg C  

Multi-step reaction with 9 steps 1: 53 percent / VO(acac)2, tert-butylhydroperoxide / benzene / 48 h / 40 °C2: 92 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature3: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature4: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux5: 58 percent / 1 h / 200 °C6: 94 percent / H2 / Pt-oxide / acetic acid / 1 h7: 62 percent / K2CO3 / 16 h / Ambient temperature8: 6 h / 60 °C9: 15 percent HCl / 1) 16 h, r.t.; 2) 30 min, 60 deg C  

Multi-step reaction with 5 steps 1: 87 percent / lithium iodide hydrate / dimethylformamide / 1 h / Heating2: 94 percent / H2 / Pt-oxide / acetic acid / 1 h3: 62 percent / K2CO3 / 16 h / Ambient temperature4: 6 h / 60 °C5: 15 percent HCl / 1) 16 h, r.t.; 2) 30 min, 60 deg C  

Multi-step reaction with 5 steps 1: 58 percent / 1 h / 200 °C2: 94 percent / H2 / Pt-oxide / acetic acid / 1 h3: 62 percent / K2CO3 / 16 h / Ambient temperature4: 6 h / 60 °C5: 15 percent HCl / 1) 16 h, r.t.; 2) 30 min, 60 deg C  

Multi-step reaction with 4 steps 1: 94 percent / H2 / Pt-oxide / acetic acid / 1 h2: 62 percent / K2CO3 / 16 h / Ambient temperature3: 6 h / 60 °C4: 15 percent HCl / 1) 16 h, r.t.; 2) 30 min, 60 deg C